Interviews with Distinguished British Chemists: Harry Emeleus (unedited footage), Tapes 1-2
- 1988-Jul-05
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Transcript
00:00:00 It's a nice view from up here, isn't it?
00:00:04 Yes, I chose this room because when I came here first, there was a Panton Brewery just
00:00:09 a hundred yards across there.
00:00:12 And I got the lovely smell of malt from here.
00:00:14 I'll bet you did.
00:00:16 I had several choices, but this was really marvelous, to have the window open in the
00:00:20 sun and get the malt smell.
00:00:21 Yes, I love it.
00:00:22 It's packed up now, but it's very, very nice.
00:00:25 I must say, the Garden House Hotel is absolutely delightful.
00:00:29 It's a beautiful hotel, and we had a very nice meal.
00:00:32 I'm going to give you a count down, and then you proceed on to the next one.
00:00:39 You don't have these papers.
00:00:41 You don't have these papers.
00:00:43 What papers?
00:00:44 These.
00:00:45 You don't see these.
00:00:46 No.
00:00:47 Oh, good.
00:00:48 Five, four, three, two.
00:00:53 Professor Emelius, can we begin by talking a little bit about your family background?
00:00:58 I know, for example, that your father led a very interesting career before he finally
00:01:03 moved to England and settled in Sussex.
00:01:06 Yes.
00:01:07 Well, as you probably know, he was a Swedish Finn, as opposed to the Finnish-speaking Finns,
00:01:16 who were the original people of Sweden, coming to the west coast of Finland and settled there.
00:01:24 It was an old family, and his father was a judge, and he died rather young.
00:01:34 My grandmother married again, and we went over there in 1909 for the first time and
00:01:41 spent the summer at the family villa out on one of the lakes.
00:01:46 After that, we had several more visits, but before the war spoiled everything and family
00:01:53 fortune went away with the upheaval of the communist regime coming into Russia, because
00:01:59 Russia owned Finland in those early days.
00:02:02 My father did his national service in the Russian army, and he qualified as a pharmacist
00:02:12 at the University of Helsinki, and he practiced for a short time.
00:02:21 But then I think he and his brothers got into some incipient political trouble, because
00:02:27 it was a fashionable thing for young Finns to be anti-Russian, and he went to sea and
00:02:34 sailed before the mast to Australia several times on Finnish ships, right round the horn
00:02:43 of the grain run, and then jumped his ship in Oregon and qualified again in pharmacy
00:02:53 at Brooklyn.
00:02:54 He'd qualified in Helsinki first, then in Brooklyn, and practiced for a short time there,
00:03:00 and came back to England and met my mother, and they were married and raised a family.
00:03:07 I was born actually in the East End of London, in Poplar, but I was taken down to Sussex,
00:03:14 and I'll tell you about that perhaps a little later, as a three-month-old infant.
00:03:20 Well, he met your mother in rather interesting circumstances, didn't he?
00:03:26 Oh yes.
00:03:27 Her father was a dock engineer in the West India docks in charge of the dock gates, and
00:03:37 they lived right on the dock.
00:03:39 And she was the secretary to Mrs Axel Lien, who ran the Scandinavian Sailors' Home.
00:03:48 Now, Mrs Lien's husband was a Swedish inventor who, among other things, provided the big
00:03:58 liners with David, launching the lifeboats, and Mother was there mixing daily with Scandinavians,
00:04:10 and she learned the three Scandinavian languages quite by ear almost, and could speak them
00:04:18 fluently.
00:04:19 And I think she and her father would have both been, in this day and age, university
00:04:26 calibre people.
00:04:27 Her father was entirely self-educated, my grandfather, and he brought himself up on
00:04:35 one of the popular self-educators of the time.
00:04:39 A real old Victorian character, a splendid old man.
00:04:43 So, after your father did get married, they eventually opened a pharmacy in Battle.
00:04:49 Yes.
00:04:50 And that pharmacy still exists today, doesn't it?
00:04:53 Oh yes, yes.
00:04:54 Yes, my brother qualified, and he took it on, and his son is now running it, and the
00:05:00 brothers retired, but are still in Battle.
00:05:03 We've still got the family connection with the old place, and it was a magnificent old
00:05:08 house, built in around 1540, with oak timbers taken from Battle Abbey.
00:05:14 It's a beautiful old place.
00:05:17 Of course, when we were kids, it was very primitive.
00:05:22 There was no plumbing in the house, and the loo was out in the backyard with a lantern
00:05:28 to get to it at night, and everything was most primitive.
00:05:33 But we had a marvellous time as kids, and very, very little money.
00:05:40 The business just about scraped by, and supported the family, but there was very, very little
00:05:47 to spare.
00:05:50 And we just lived in the country.
00:05:52 There were no bicycles.
00:05:54 We walked everywhere.
00:05:55 Thirty miles a day, there was nothing, and we fished in the local little brooks.
00:06:03 I remember well catching my first trout.
00:06:07 It was just a marvellous upbringing, which has had a profound effect on my whole life
00:06:12 ever since, you know.
00:06:15 I have always, always loved the country, and I think, in a sense, have lived in town under
00:06:21 protest.
00:06:22 And having settled down, you were not the first child, of course.
00:06:26 You have an older brother.
00:06:27 No.
00:06:28 I had a...
00:06:29 My brother, George, he's still with us, and he and I went to Hastings Grammar School.
00:06:37 That was about five to seven miles away.
00:06:40 I used to go there by train each day and back.
00:06:42 And as was the case with those old grammar schools, the teaching was marvellous.
00:06:51 And I think we both got interested in science because it was a good science teaching.
00:06:58 My brother went to Cambridge.
00:07:01 He got a scholarship at St. John's and read physics, and then went on to do a PhD with
00:07:08 Rutherford and CTR Wilson, and subsequently ended up as Professor of Physics at Belfast,
00:07:16 Queen's University Belfast.
00:07:18 And he is still living over there now.
00:07:23 And I know I tried two years after him to get a scholarship at St. John's.
00:07:27 They wouldn't have me, which I think, in retrospect, was a blessing in disguise.
00:07:33 I went then to Imperial College and got a small exhibition there.
00:07:39 And thanks to the sacrifices made by my parents, I was able to qualify to get my degree there.
00:07:48 You said you had very good science teaching at school.
00:07:51 Can you remember any teacher in particular from those early days who perhaps inspired you?
00:08:00 My chemistry teacher was Mr. Ernest Hole, H-O-L-E.
00:08:05 He was a splendid teacher.
00:08:07 And it is amazing what a difference good teaching can make.
00:08:13 I fear that educationists have now got their teeth into the educational system.
00:08:20 And in some ways, they're spoiling it.
00:08:22 You don't get that very, very fine personal attention to youngsters.
00:08:27 And did he have a large class with the many students taking chemistry or science or whatever it was?
00:08:33 Well, it was a little bigger than now, I should think.
00:08:38 I couldn't give you the size of the class.
00:08:41 But in my last year, I had a free hand of the laboratory.
00:08:45 And I did a lot of work then which would otherwise have been done at Imperial College in my first year.
00:08:53 We had a chemical balance which was really reliable to a tenth of a milligram.
00:09:01 It meant I could do all the standard gravimetric analysis up to university standard.
00:09:07 And I did a lot of that.
00:09:09 And of course, it was an enormous benefit.
00:09:12 We had all the usual sports.
00:09:15 I played cricket and I played soccer and I played hockey, field hockey.
00:09:21 And I was reasonably proficient.
00:09:24 But when I got to college, I just worked.
00:09:28 There was no...
00:09:30 I was getting, every Monday morning, two pound notes arrived with a lovely letter from my mother.
00:09:37 And that was my ration for the week.
00:09:40 I managed everything on that.
00:09:42 And so it was quite difficult when you were going to university then.
00:09:45 I mean, you had to be extremely frugal.
00:09:47 Well, there was nothing like the public support for me, you see.
00:09:52 You had to do it the hard way.
00:09:55 And, golly, I learned a lot from that.
00:09:58 It was useful because in later years I met lots and lots of hard-up students
00:10:04 and I think I had a feeling for them which I wouldn't have had
00:10:07 if I'd been rather better cushioned in the early days.
00:10:12 Was it always expected by, say, your father or your mother
00:10:16 that you would, say, go into pharmacy or go into the family business?
00:10:21 Or did you always know that you were going to go into science of some sort?
00:10:26 Because it seems to have always been that you were doing science from a very early age
00:10:30 and there was no question in your mind that science was where your interests lay.
00:10:33 Well, in a way, my chemistry started at home.
00:10:38 I used to mix up horse medicines and make pills.
00:10:43 Quite a lot of these operations, of course, were done then.
00:10:46 It was way before the days of very mixed-up medicines.
00:10:52 The pharmacist was the local vet and people came to him
00:10:57 and he dispensed all his own mixtures for them for the various ailments.
00:11:01 I mixed not for humans but for animals.
00:11:04 I trusted with making things like that.
00:11:07 Oh, and in my early teenage,
00:11:10 I can remember with a pair of old pharmacist scales,
00:11:15 being precise in my weighing was something that mattered to me.
00:11:20 But I think father had the ambition that we would,
00:11:23 my brother and I, would go to Heidelberg.
00:11:26 And, of course, when the time came, we should have gone
00:11:29 and family money was all disappeared.
00:11:32 His eldest son would have been reasonably well off from the Finnish estate
00:11:36 but that all disappeared and we had to do it for ourselves,
00:11:43 which, just fair enough, that's the way it came.
00:11:48 He had a great ambition for us, but never to be pharmacists.
00:11:54 He wanted us to get into the academic world.
00:11:58 And your mother?
00:12:00 Well, she was a magnificent person, absolutely marvellous.
00:12:04 She kept the whole thing going.
00:12:06 We had a lovely home life and she,
00:12:10 well, somehow she managed to keep the business solvent
00:12:16 on post-dated cheques.
00:12:19 And the result was that home was just what it always should be.
00:12:26 And so she provided the sort of very comfortable background
00:12:31 This time there were five of you.
00:12:33 You had sisters and brothers.
00:12:35 Can you tell us a little bit about your other brothers
00:12:38 and your other members of your family?
00:12:40 Well, one brother went to Cambridge
00:12:43 and the second qualified in pharmacy
00:12:48 and took over the business.
00:12:51 And the two sisters,
00:12:54 one didn't marry, she helped with the pharmacy,
00:12:58 and the other married a man
00:13:01 who joined the Black Watch in the First War of 16
00:13:04 and had been badly smashed up,
00:13:06 and they had a chicken farm.
00:13:10 He was a pretty good chap,
00:13:14 but, golly, he had a bad, rough time.
00:13:17 That was the family.
00:13:19 We were all very, very much a unit
00:13:21 and four of us are still alive,
00:13:24 so we're very blessed.
00:13:26 And when you went to university,
00:13:30 it was not known as Imperial College in those days, was it?
00:13:33 It was the Royal College of Science
00:13:36 and there were the three colleges
00:13:40 which were separate.
00:13:43 There was City and Guild Engineering College,
00:13:45 the Royal School of Mines,
00:13:46 and the Royal College of Science.
00:13:48 And I took my degree,
00:13:52 I took the Associateship of the Royal College of Science
00:13:55 and then had to take the external London BSc
00:13:59 in the following September.
00:14:01 I think that was the last or the next to last year
00:14:05 when that old system had to maintain.
00:14:12 One or two years after that
00:14:16 it was possible to take the London BSc automatically
00:14:20 on the strength of the results of the college exam.
00:14:24 And then some years later
00:14:26 it became the Imperial College
00:14:29 with one administration.
00:14:32 And what was the college like when you went to it?
00:14:34 What was life like as a student
00:14:36 back in London in those days?
00:14:39 Well, I lived in a bedsit.
00:14:41 I had a thoroughly miserable time.
00:14:44 Well, if it had been for the work
00:14:46 I'd have been miserable,
00:14:48 there was hardly any recreation.
00:14:52 Occasionally to the Old Vic,
00:14:54 the gallery for sixpence.
00:14:56 Can you remember anything you saw at the Old Vic?
00:14:59 Why, yes.
00:15:00 I saw most of the Shakespeare's
00:15:02 and there was opera there too.
00:15:05 And I got a pretty good dose of it.
00:15:09 That went right through my time in London
00:15:11 when I was even doing postgraduate work.
00:15:14 And when you were doing your undergraduate work
00:15:17 you began some research projects.
00:15:20 You had a particular project
00:15:22 into a research project.
00:15:24 Not, you see,
00:15:26 I'd done enough at school
00:15:29 under those post-war conditions
00:15:32 to take my final exam in two years.
00:15:36 And then I went straight into research.
00:15:39 And
00:15:43 there was no research project
00:15:45 which was part of the undergraduate course.
00:15:48 And what was the first research project
00:15:50 you did undertake?
00:15:52 Oh, that was rather a joke really.
00:15:57 The professor of inorganic chemistry,
00:16:02 I think I went to him because I liked his lectures.
00:16:07 I had a choice.
00:16:08 I could have gone to physical or to organic chemistry.
00:16:11 And neither attracted me particularly
00:16:14 but inorganic I liked the lectures
00:16:17 with the demonstrations in the lectures.
00:16:20 And H.P. Baker was the professor.
00:16:26 He was a very interesting old gentleman
00:16:30 because when one went to ask him about research
00:16:34 the one thing he was fatal to do
00:16:36 was to say he wanted to get a PhD.
00:16:40 With him one did research for its own sake.
00:16:43 No half measure at all.
00:16:45 And I think I said all the right things
00:16:49 because he accepted me.
00:16:51 And the question arose obviously
00:16:54 what I was going to do.
00:16:56 And he said he thought he had a problem
00:16:57 that would interest me
00:16:58 which was to study
00:17:00 whether platinum would be attacked by bromine
00:17:05 under the influence of rays from radium
00:17:10 that was the phrase he used.
00:17:13 Well of course my next question was
00:17:15 where's the radium?
00:17:16 And he went into his old desk
00:17:18 which was horribly untidy
00:17:21 and scuffled around
00:17:22 and finally he produced a piece of lead
00:17:25 with a small open tube
00:17:27 which was violet in colour
00:17:29 and he said that was the radium.
00:17:30 Now nobody knew how much that was
00:17:33 I think it was an old sample he'd got from France
00:17:37 in the old days of radium.
00:17:39 And I was left to devise an experiment
00:17:43 I sealed this
00:17:48 tried to seal this up in vacuum
00:17:51 with a bit of bromine
00:17:52 and a weighed piece of platinum
00:17:54 and the radium tube inside
00:17:56 and the problem was to evacuate it.
00:17:58 We had no oil pumps to evacuate the tube
00:18:01 so we had a water pump
00:18:03 attached to a water pump
00:18:04 went away to lunch
00:18:05 and someone turned off the water pump
00:18:06 and flooded the whole thing
00:18:07 radium and oil.
00:18:08 So that was absolutely disastrous
00:18:10 and of course I had to tell him
00:18:13 I don't think he was very pleased
00:18:16 it didn't really hit the ceiling
00:18:18 but I think he did it after I'd left him
00:18:21 and I went through the motions
00:18:25 of recovering the radium
00:18:26 by adding barium
00:18:27 and precipitating barium sulphate
00:18:30 I presented him with a very clean white sample
00:18:33 which I told him would contain his radium
00:18:36 no one knew what was lost
00:18:39 or what the quantities were at all
00:18:43 so that was my first research
00:18:46 and after that
00:18:48 that dear old gentleman
00:18:50 never suggested anything else for me
00:18:54 he left me to find my own research projects
00:18:57 which was alright to start with
00:19:01 but the thing was
00:19:03 what I did
00:19:05 I was encouraged to publish
00:19:06 entirely in my own name
00:19:07 and of course
00:19:08 those first few years of research
00:19:10 if one can publish independently
00:19:12 it's absolutely critical
00:19:14 to getting established
00:19:16 you have to choose the right things to do obviously
00:19:19 but I was attracted
00:19:22 by a phenomenon
00:19:24 which then was known as
00:19:25 the glow of phosphorus
00:19:27 the chemiluminescent oxidation
00:19:29 and
00:19:31 I
00:19:34 had seen this demonstrated
00:19:36 in Baker's lectures
00:19:38 and there was various facets
00:19:40 of that problem
00:19:41 there was no theory of chain reactions
00:19:43 in those days
00:19:44 it was all
00:19:46 just trying to explain a phenomenon
00:19:48 and I made some
00:19:50 I suppose quite interesting studies
00:19:52 including
00:19:54 photographing the spectrum
00:19:56 of the glow of phosphorus
00:19:57 with a very small aperture
00:19:59 spectroscope
00:20:00 quartz spectroscope
00:20:01 and observing for the first time
00:20:03 the lovely set of bands
00:20:05 in the infrared
00:20:07 in the ultraviolet spectrum
00:20:09 of the emission spectrum
00:20:11 it
00:20:13 it was quite a
00:20:15 quite a nice project
00:20:17 and it gave me my first publications
00:20:19 and then I went on
00:20:21 from that to study
00:20:23 the low temperature oxidation of sulfur
00:20:25 and arsenic
00:20:27 and of ether
00:20:29 and those three things together
00:20:31 gave me my doctor of science thesis
00:20:33 which you got in which year
00:20:35 I got that after I had been to Germany
00:20:37 yes
00:20:39 you actually had a PhD
00:20:41 before you had your doctor of science
00:20:43 you did get the PhD
00:20:45 even if Baker had not encouraged you
00:20:47 to work towards it necessarily
00:20:49 well that came in one stride
00:20:51 yes
00:20:53 I think it must have been
00:20:55 yes I was three years before the PhD
00:20:57 including the first year
00:20:59 I might have been undergraduate
00:21:01 and I had then
00:21:03 I was still very hard up then
00:21:05 because the
00:21:07 the grants from the government
00:21:09 were not anything like as generous
00:21:11 as they are now
00:21:13 but your fortunes changed a little bit
00:21:15 when you did decide to go to Germany didn't they
00:21:17 although actually you had a choice of going to
00:21:19 you were going to go abroad
00:21:21 from you
00:21:23 no they changed when
00:21:25 I got a
00:21:27 a senior exhibition
00:21:29 1841
00:21:31 1851 sorry
00:21:33 that was for those days
00:21:35 it was a very very
00:21:37 nicely funded
00:21:39 scholarship
00:21:41 I think it brought in 450 pounds a year
00:21:43 which was marvellous
00:21:45 and
00:21:47 Baker advised me to go abroad
00:21:49 and
00:21:51 he and Sidgwick
00:21:53 interviewed me
00:21:56 and Baker wanted me to go to Paris
00:21:58 to
00:22:00 a Frenchman, Lebeau
00:22:02 who'd been one of Moisson's assistants
00:22:04 in the field of fluorine chemistry
00:22:06 and Sidgwick wanted me to go
00:22:08 to Alfred Stock
00:22:10 who worked on silicon
00:22:12 and germanium hydrides
00:22:14 Stock was then
00:22:16 he'd just moved to Karlsruhe
00:22:18 and
00:22:20 because that was a
00:22:22 black
00:22:24 that's
00:22:26 that's a real pyramid
00:22:28 yes
00:22:30 yes
00:22:42 well Stock had just been
00:22:48 diagnosed as suffering from mercury poisoning
00:22:50 and he was just scared of it
00:22:52 and got a lot of mercury
00:22:54 into his system
00:22:56 and I used to do mercury analyses
00:22:58 on his urine
00:23:00 and this is hard to believe
00:23:02 but from one litre of urine
00:23:04 one could get a visible
00:23:06 droplet of metallic mercury
00:23:08 so he really had
00:23:10 bad effects of it
00:23:12 that was a thing
00:23:14 in the lab
00:23:16 but my social life was
00:23:18 very much
00:23:20 that of the assistant
00:23:22 we had our coffee parties
00:23:24 and we went up
00:23:26 I didn't do any skiing
00:23:28 that was the one thing I missed
00:23:30 we were just on the edge of the black forest
00:23:32 I didn't ski but we made a lot of trips
00:23:34 into the black forest
00:23:36 at weekends together
00:23:38 and I swam in the Rhine
00:23:40 which was then not too dirty
00:23:42 mostly work
00:23:44 I'm afraid I was addicted to that
00:23:46 in those times too
00:23:48 one and a half years
00:23:50 and then what did you do after that?
00:23:52 I went back then and finished my Doctor of Science degree
00:23:54 and the question was
00:23:56 what would I do
00:23:58 go into industry or teach
00:24:00 or go on
00:24:02 and luckily
00:24:04 I
00:24:06 chose to go on
00:24:08 and I had an interview
00:24:10 with ICI
00:24:12 in Billingham
00:24:14 they offered me 500 a year to go there
00:24:17 and I turned that down
00:24:19 and I got an American scholarship
00:24:21 which was very generous
00:24:23 and took me to Princeton
00:24:25 that was the
00:24:27 scholarship funded by the Harkins Foundation
00:24:29 of New York
00:24:31 and it was called a Commonwealth Fund Fellowship
00:24:33 and we
00:24:35 had
00:24:37 two
00:24:39 years
00:24:41 and I worked with H.S. Taylor
00:24:43 the physical chemist at Princeton
00:24:45 and in my
00:24:47 vacations I had an obligation to travel
00:24:49 which meant I saw a lot of
00:24:51 states
00:24:53 How did you travel to the United States
00:24:55 at that time
00:24:57 when you first left England
00:24:59 was it by sea?
00:25:01 Oh yes
00:25:03 those were the days
00:25:05 you might say
00:25:07 I was with
00:25:09 two other Commonwealth Fellows
00:25:11 we had a very good party on board
00:25:13 What were their names?
00:25:15 Eric Ashby
00:25:17 he is now
00:25:19 a peer of the realm
00:25:21 he was a botanist
00:25:23 from Imperial College
00:25:25 and he was going out
00:25:27 as a Commonwealth Fund Fellow
00:25:29 to go to Hawaii
00:25:31 I think he was working on tropical agriculture
00:25:33 seemed a very delectable
00:25:35 place to go to
00:25:37 then
00:25:39 Monty Barrack
00:25:41 he was
00:25:43 a fellow chemist from Oxford
00:25:45 he was a New Zealander
00:25:47 and I did a big travel with him
00:25:49 in the
00:25:51 long vacation between my two years
00:25:53 we had a car
00:25:55 and camping gear
00:25:57 went right across to the Rockies
00:25:59 and spent
00:26:01 about two months
00:26:03 in the Rockies in the wilds
00:26:05 camping and climbing and fishing
00:26:07 very good going
00:26:09 Can you tell us what life was like
00:26:11 in Princeton
00:26:13 for people coming from
00:26:15 England in those days
00:26:17 Well I think for me
00:26:19 it was totally new
00:26:21 because I had been
00:26:23 living in bed sit accommodation
00:26:25 in London
00:26:27 which was not at all good
00:26:29 and there I lived in the graduate
00:26:31 college at Princeton
00:26:33 and it was marvellous
00:26:36 we had a couple of very nice rooms
00:26:38 the grad college is out on the
00:26:40 golf links
00:26:42 we worked hard
00:26:44 I had a car to drive
00:26:46 and
00:26:48 we had reasonable social life
00:26:50 very much like Cambridge College
00:26:52 and
00:26:54 swimming
00:26:56 skating
00:26:58 we even had an 8 on the river
00:27:00 on the lake, on Lake Carnegie
00:27:02 that was
00:27:04 we were coached by
00:27:06 Bob Spence who
00:27:08 later on was
00:27:10 at Harwell
00:27:14 he was a Durham
00:27:16 oarsman
00:27:18 and at one time we had 7 nationalities
00:27:20 in our 8
00:27:22 in the graduate college
00:27:24 it was very nice
00:27:26 one of them was Wegener
00:27:28 a very notable
00:27:30 physicist
00:27:32 who later on developed
00:27:34 studied
00:27:36 a phenomenon known as the Wegener effect
00:27:38 but it really
00:27:40 was my first touch
00:27:42 of proper social life
00:27:44 in the university
00:27:46 and you took up folk dancing
00:27:48 well I met my wife on folk dancing
00:27:50 my future wife
00:27:52 and
00:27:54 we went down for two trips
00:27:56 to New York
00:27:58 with a Princeton team
00:28:00 and
00:28:04 we were married
00:28:06 the day before I sailed
00:28:08 to the little church around the corner in New York
00:28:10 which was rather
00:28:12 a well known place over there
00:28:16 your wife's name was
00:28:18 Catherine Horton
00:28:20 she was from Virginia wasn't she
00:28:22 yes, from Lynchburg
00:28:26 and you weren't allowed to
00:28:28 be married
00:28:30 so you actually had to wait
00:28:32 I had to wait yes
00:28:34 I was allowed one day
00:28:36 but it was
00:28:38 she was working
00:28:40 as a secretary to the librarian
00:28:42 at Princeton
00:28:44 so it was very
00:28:46 obviously near neighbours
00:28:48 and
00:28:50 everything worked out very nicely
00:28:52 what did you work on
00:28:54 what sorts of problems were you working on in Princeton
00:28:57 well Taylor was
00:28:59 interested in photochemistry
00:29:01 and I worked on the photochemistry
00:29:03 of ammonia
00:29:05 and amines
00:29:07 and the polymerisation of olefins
00:29:09 in presence of the radiated ammonia
00:29:11 and amines
00:29:13 it made quite a
00:29:15 new field for me
00:29:17 facilities were very good
00:29:19 and I got three or four publications
00:29:21 with H.S. Taylor
00:29:23 to show for my time
00:29:25 and when you and your
00:29:27 wife left New York
00:29:29 to go to England
00:29:31 did she expect that she was going
00:29:33 to settle here, I mean did it ever occur
00:29:35 to you that you might settle in the United States
00:29:37 well I came home
00:29:39 without a job
00:29:41 that was a poor start
00:29:43 I got one
00:29:45 £300 a year at Imperial College
00:29:47 which was less than she had been earning
00:29:49 in Princeton
00:29:51 and we settled down
00:29:53 in a very scruffy
00:29:55 little
00:29:57 ground floor flat
00:29:59 in Battersea
00:30:01 just off the park
00:30:03 that was
00:30:05 pretty much to ask of her
00:30:07 but she was a good
00:30:09 pioneer spirit, she stuck it
00:30:11 and it worked out gradually
00:30:15 I got a job at Imperial College
00:30:17 in the lowest
00:30:19 bracket
00:30:21 and I was very glad of it
00:30:23 so what were you working on
00:30:25 at Imperial College
00:30:27 I had
00:30:29 I was on my own
00:30:31 that's important
00:30:33 and I did a mixture
00:30:35 of things
00:30:37 I had the experience of physical chemistry
00:30:39 with Taylor
00:30:41 I had one or two projects in physical chemistry
00:30:45 but one of the main things I
00:30:47 developed was an interest in
00:30:49 hydride chemistry where I could
00:30:51 use the Stok technique
00:30:53 because that technique
00:30:55 was brand new in England
00:30:57 no one had ever had it before
00:30:59 and I was able to develop that
00:31:01 for the first time
00:31:03 and it gave me a very
00:31:05 good
00:31:07 line because
00:31:13 I think it was a
00:31:15 I was interested in preparative chemistry
00:31:18 and I gradually dropped the physical chemistry
00:31:20 and got more and more
00:31:22 into preparative chemistry
00:31:26 you see
00:31:28 you really have to remember
00:31:30 that chemistry wasn't
00:31:32 developed in anything
00:31:34 like the degree it is now
00:31:36 all of the modern things
00:31:38 like NMR, spectroscopy, infrared
00:31:40 and even x-ray work
00:31:42 was
00:31:44 only just beginning
00:31:46 and there wasn't a lot to do
00:31:48 in inorganic
00:31:50 except preparative work
00:31:52 and the
00:31:54 field was absolutely enormous
00:31:56 anyone with any sort of imagination
00:31:58 could pick up a journal
00:32:00 and get
00:32:02 absolutely unlimited
00:32:04 ideas for worthwhile new research
00:32:06 and there was
00:32:08 hardly any competition
00:32:10 there was a certain amount
00:32:12 of good manners
00:32:14 I remember writing
00:32:16 to somebody in Germany
00:32:18 very apologetically and saying
00:32:20 would he mind if I did so and so
00:32:22 because he had shown some interest in it
00:32:24 that was the norm then
00:32:26 but it really was
00:32:28 a pretty wide open field
00:32:30 and with the silicon hydride
00:32:32 one of the things
00:32:34 my students made
00:32:36 was the
00:32:38 silicon analogue of methyl iodide
00:32:40 SiH3I
00:32:42 which of course
00:32:44 is a
00:32:46 opens up the whole field of
00:32:48 organometallics
00:32:50 using silicon
00:32:52 SiH3
00:32:54 instead of CH3
00:32:56 and we took that and we made
00:32:58 a lot of
00:33:00 derivatives
00:33:02 that and with the methyl silanes
00:33:04 and
00:33:06 extended
00:33:08 that also to some
00:33:10 chemical work on SiH3
00:33:12 gradually you see built round
00:33:14 into the preparative side
00:33:16 as opposed to the physico-chemical
00:33:18 and that's what
00:33:20 became known for
00:33:22 I had a very small number of research students
00:33:24 but they were very good
00:33:26 and that went on
00:33:28 until the war years
00:33:30 and did you have
00:33:32 many
00:33:34 publications
00:33:36 you were opening up this field at this time
00:33:39 so you must have had lots of
00:33:41 publications
00:33:43 yes I think
00:33:45 I couldn't give you numbers
00:33:47 but they were half a dozen
00:33:49 a year that was the sort of output
00:33:51 which was in keeping
00:33:53 with the size of our group
00:33:55 and was your
00:33:57 financial position improving
00:33:59 were you still in the scruffy flats in Battersea
00:34:03 we gradually got
00:34:05 a little bit better
00:34:07 it wasn't a lot
00:34:09 but it was some of it
00:34:11 and
00:34:13 I couldn't tell you
00:34:15 when the first youngsters was born
00:34:17 it must have been
00:34:19 you see I took my job there
00:34:21 in 1931
00:34:23 must have been 1935 or thereabouts
00:34:25 we got then into a better flat
00:34:27 and moved out to
00:34:29 Turn Green
00:34:31 and
00:34:33 that's where
00:34:35 we were when the war started
00:34:37 and when the war started
00:34:39 you
00:34:41 didn't want your wife to stay up in London
00:34:43 so your wife actually
00:34:45 moved down to live with your family in Battle
00:34:47 didn't she?
00:34:49 she took a small house on the outskirts of Battle
00:34:51 and I
00:34:53 went to live
00:34:55 in college
00:34:57 had a room in the
00:34:59 college union
00:35:01 and
00:35:03 you possibly know that Imperial College
00:35:05 was
00:35:07 the only London college which did not
00:35:09 evacuate itself to the
00:35:11 provinces
00:35:13 we went on with our teaching
00:35:15 and the research was switched over
00:35:17 to special research for the
00:35:19 ministry
00:35:21 and did
00:35:23 life go on as usual in the lab
00:35:25 during the war?
00:35:27 it must have been very difficult sometimes
00:35:29 you mean
00:35:31 well yes you were involved
00:35:33 in some work
00:35:35 associated with air raids
00:35:37 right?
00:35:39 well
00:35:41 there were several parallel things
00:35:43 going on
00:35:45 let me talk about the work first
00:35:47 the work was
00:35:49 mostly
00:35:51 work that was secret
00:35:53 and was
00:35:55 for the ministry of supply
00:35:57 and
00:36:00 we were asked to investigate
00:36:02 the
00:36:04 preparation properties of a range
00:36:06 of very
00:36:08 aggressive
00:36:10 but little known
00:36:12 fluorine compounds
00:36:14 the problem was
00:36:16 would they be used by the Germans as war gases
00:36:18 and these
00:36:20 compounds included bromine
00:36:22 and fluorine
00:36:24 iodine fluoride
00:36:26 and things of that sort
00:36:28 which were very
00:36:30 toxic
00:36:32 and we had the experience
00:36:34 of preparative chemistry
00:36:36 and we made these
00:36:38 and we had
00:36:40 white rats kept in the building
00:36:42 for preliminary
00:36:44 toxicity tests
00:36:46 and then we worked closely
00:36:48 in connection with the port
00:36:50 experimental station
00:36:52 chemical defence station
00:36:54 so that was really the work
00:36:56 again about half a dozen
00:36:58 they could do their PhD's on the basis
00:37:00 of that secret work
00:37:02 much of which was never published
00:37:04 excepted by the university
00:37:06 and
00:37:08 the other things
00:37:10 I did
00:37:12 rather a joke I had a commission
00:37:14 in the home guard
00:37:16 and
00:37:18 then ERH Jones
00:37:20 and I were both
00:37:22 as advised
00:37:24 in fairly senior positions
00:37:26 we lectured to
00:37:28 gas identification officers
00:37:30 on a regular basis
00:37:32 at the college
00:37:34 I think
00:37:36 I think that was
00:37:38 about all we had
00:37:40 because nothing happened
00:37:42 the only major alarm
00:37:44 we had was when
00:37:46 the white solid substance was
00:37:48 found in the roadway at Marble Arch
00:37:50 and we were
00:37:52 Jones and I were rushed up there
00:37:54 with a police escort to identify it
00:37:56 because there had been a scare
00:37:58 about solid arsenic compounds
00:38:00 and this proved to be snow
00:38:02 from a barrage balloon
00:38:04 the whole of Marble Arch was stood to stand
00:38:06 until we gave it a little clear
00:38:08 but that was the sort of
00:38:10 one-off
00:38:12 there was really very little
00:38:14 with the gas job again
00:38:16 What did you do during air raids?
00:38:18 Oh well there I was
00:38:21 in charge of the
00:38:23 firefighting for the college
00:38:25 and